Experimental Investigation on Entrainer / Solvent Performance for Acetone – Chloroform, Acetone – Methanol and Benzene – Cyclohexane Systems

International Journal of Advanced Research in Engineering and Technology (IJARET), 11(3), 2020, pp 390-399

10 Pages Posted: 28 Apr 2020

See all articles by B. Sivaprakash

B. Sivaprakash

Associate Professor, Department of Chemical Engineering, Annamalai University, Annamalainagar, India

R. Ramsenthil

Associate Professor, Department of Chemical Engineering, Annamalai University, Annamalainagar, India

M.S. Manojkumar

Assistant Professor, Department of Petrochemical Engineering, Mahendra Institute of Engineering and Technology, Namakkal, India

Date Written: April 3, 2020

Abstract

Azeotropes are commonly occurring phenomena in distillation operations that leads to complexity in separation of the components. Azeotropes are due to excessive positive or negative deviation from ideality. They require a key component called entrainer to separate them. In the present study three azeotropic systems namely Acetone - Chloroform, Acetone - Methanol and Benzene - Cyclohexane were investigated experimentally to identify the performance of entrainers in separating them using azeotropic distillation. The experiments were conducted using an Othmer VLE still and the results are presented. Based on the experimentations it was found that water (entrainer) gave the best recovery for the acetone - chloroform and acetone - methanol systems and chlorobenzene yielded more separation for the benzene - cyclohexane system.

Keywords: azeotropic systems, entrainer, chlorobenzene

Suggested Citation

Sivaprakash, B. and Ramsenthil, R. and Manojkumar, M.S., Experimental Investigation on Entrainer / Solvent Performance for Acetone – Chloroform, Acetone – Methanol and Benzene – Cyclohexane Systems (April 3, 2020). International Journal of Advanced Research in Engineering and Technology (IJARET), 11(3), 2020, pp 390-399, Available at SSRN: https://ssrn.com/abstract=3567707

B. Sivaprakash (Contact Author)

Associate Professor, Department of Chemical Engineering, Annamalai University, Annamalainagar, India ( email )

Annamalainagar
Annamalai University
Chidambaram, TN Tamil Nadu 608002
India

R. Ramsenthil

Associate Professor, Department of Chemical Engineering, Annamalai University, Annamalainagar, India ( email )

Annamalainagar
Annamalai University
Chidambaram, TN Tamil Nadu 608002
India

M.S. Manojkumar

Assistant Professor, Department of Petrochemical Engineering, Mahendra Institute of Engineering and Technology, Namakkal, India ( email )

Namakkal
TN
India

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